How to use rotary evaporator?
Rotary Vacuum Evaporator Description:
Rotary evaporator is one of the indispensable equipment for experiments in the laboratory, which consists of heating tub, evaporating flask, condenser tube, and so forth. By controlling, the evaporating flask is constantly rotated at an applicable rotation speed, and the evaporating flask is positioned in a heating bathtub to carry out constant temperature heating while rotating, thereby uniformly heating the response solvent within the evaporating flask. During rotation, the response medium adheres to the walls of the evaporating flask, which increases the evaporation space. Use a circulating water vacuum pump to maintain the evaporating flask in a unfavorable pressure state, cut back the evaporation temperature of the answer within the evaporating flask beneath the unfavorable stress state, and pace up the evaporation fee. The coils of the high-efficiency cooler cross with the cooling medium to liquefy the distillate vapor for separation.
The rotary evaporator rotates at a continuing velocity under constant temperature heating and vacuum circumstances, so that the reaction solvent varieties a film on the wall of the rotating bottle. After efficient evaporation, the solvent is cooled and recovered by a glass condenser, which might effectively enhance the work efficiency. At current, the rotary evaporator isn’t only an instrument and equipment in most scientific analysis laboratories similar to food, medicine, biology, etc., however is mainly used for material concentration, crystallization, drying, separation, solvent recovery and extraction (such as for the extraction of celery leaf important oil.
The following points can be used as the premise for you to select and purchase a rotary evaporator:
Confined house of rotary evaporator
The closed house of the rotary evaporator consists of glass parts such as evaporating bottle, receiving bottle, sealing ring, condenser tube, vacuum buffer bottle, vacuum pump and vacuum pipeline. Among these elements, the vacuum diploma of the entire system is especially critical and shall be affected by the surface world. The variable factors are: vacuum pump, seals and vacuum tubes.
Lifting method of rotary evaporator
Lifting strategies are divided into manual lifting and computerized lifting, and automatic lifting is also divided into: automatic lifting of water tub and automatic lifting of evaporating bottle. Automatic lifting rotary evaporator is principally appropriate for many who use it regularly, and automatic lifting saves somewhat effort. In reality, some great benefits of water bath lifting: it might possibly protect the evaporating bottle, the glass shaft just isn’t straightforward to be broken, and manual lifting is extra economical than automatic lifting, such because the RE-201D small-capacity rotary evaporation produced and bought by our company. The instrument is very cost-effective!
Sealing diploma of rotary evaporator:
Look on the sealing degree of the rotary evaporator, that’s, the vacuum diploma. The higher the vacuum degree, the sooner the evaporation fee. Generally, the vacuum diploma can attain zero.095mpa. Generally, 2L and 5L may be equipped with a desktop circulating water vacuum pump, and a vertical circulating water vacuum pump must be outfitted with a 10L or extra. The degree of vacuum additionally has so much to do with the sealing ring. Generally, the standard of the sealing ring is good. Some are extra corrosion-resistant, in order that any flux won’t have an effect on the vacuum pump, and the service life is relatively long. In phrases of the vacuum diploma in the rotary evaporator, the recommended vacuum diploma in the industry is 95~98kPa; in phrases of the temperature of the cooling medium of the condenser, the relationship between the material temperature and the vacuum diploma is in line with the relationship between the fabric saturation temperature and the saturation strain. When the temperature and vacuum diploma are determined, the temperature of the cooling medium is decided by the kind of materials.
Specifications of Rotary Evaporator
The specifications of the rotary evaporator are often distinguished by the quantity of the evaporating flask, and its size depends on the amount of the material to be evaporated. In basic, 1L, 2L, 3L, and 5L rotary evaporators are suitable for small pattern check in laboratory; 5L, 10L, and 20L are suitable for pilot check; 20L and 50L are appropriate for pilot take a look at and production.
Distillation effectivity of rotary evaporator
The distillation efficiency of the rotary evaporator determines the output. In the case of the identical solvent, the higher the distillation effectivity, the larger the number of samples to be distilled. If the pattern volume is large, it is needed to choose the best one by way of distillation efficiency.
Security danger evaluation
If the distillation solvent is flammable and explosive, the rotary evaporator with explosion-proof glass parts is principally selected. In order to optimize the laboratory environment, a secondary condensing device can also be chosen to maximize the recovery of the distillation solvent.
Compare, did you choose the proper one?
The description of rotary vacuum evaporator is here. The subsequent article will introduce rotary evaporator uses in industry intimately.
In addition, if you wish to buy a rotary evaporator, whether or not it is a large-capacity rotovap machine or a small-capacity rotary evaporator (such as re 501 rotary evaporator), be certain to contact us in time! We will provide you with a quote that can fulfill you!
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